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EBSD coupled to SEM in-situ annealing as a tool to identify recrystallization mechanisms - Application to Zr and Ta alloys

Abstract : A heating stage as been developed to perform in-situ annealing in a SEM equipped with an EBSD system in order to study recrystallization mechanisms. High temperature treatments could then be performed inside the SEM, up to 1180°C and with high heating- and cooling-rates (∼100°C.s -1). Samples were cooled down to room temperature to perform EBSD orientation mapping in between successive short-duration heat-treatments. Microstructure evolution snapshots obtained this way are presented in this paper to show recrystallization in Zircaloy4 and in pure tantalum.
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Submitted on : Wednesday, May 23, 2012 - 4:59:37 PM
Last modification on : Wednesday, March 17, 2021 - 5:20:03 PM

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Nathalie Bozzolo, Suzanne Jacomet, Marie Houillon, Benoît Gaudout, Roland E. Logé. EBSD coupled to SEM in-situ annealing as a tool to identify recrystallization mechanisms - Application to Zr and Ta alloys. 4th International Conference on Recrystallization and Grain Growth, ReX and GG IV, Jul 2010, Sheffield, United Kingdom. pp.Pages 486-491, ⟨10.4028/www.scientific.net/MSF.715-716.486⟩. ⟨hal-00700726⟩

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